在本研究中,先在预磨机上进行预磨,然后在150、320、600和1000号砂纸上依次水磨,在抛光机上进行机械抛光,抛光后的试样置于4 ml 硝酸(HNO3) + 96 ml 无水乙醇(CH3CH2OH)混合溶液浸蚀10~20 s,在Olympus GX53光学显微镜中观察300℃ 、400℃以及500℃保温15min的金相组织,微观组织没有明显变化,为粒状贝氏体,而在600℃下保温15min的金相组织,微观组织中岛状颗粒发生分解,在700℃下保温15min的金相组织,微观组织中岛状颗粒完全分解。
In this study, pre-grinding was carried out on a pre-grinding machine, and then water grinding was carried out on sand paper 150, 320, 600 and 1000 in turn, and mechanical polishing was carried out on a polishing machine. After polishing, the sample was immersed in a mixed solution of 4 mL nitric acid (HNO3) + 96 mL anhydrous ethanol (CH3CH2OH) for 10~20 s. When observed in Olympus GX53 optical microscope at 300℃, 400℃ and 500℃ for 15min, the microstructure showed no obvious change and was granular bainite, while when held at 600℃ for 15min, the island particles in the microstructure decomposed. After holding for 15min at 700℃, the island particles in the microstructure were completely decomposed.