采用X射线衍射仪(XRD,日本 Rigaku,D/max 2500PC)分析粉末和涂层的物相组成。具体测试参数:Cu靶Ka辐射,特征波长λ=0.154056 nm,衍射角(2θ)扫描速度为0.02 °/s,扫描范围为20 °- 80 °,电流为100 mA,电压为40 KV。
The phase composition of powder and coating was analyzed by X-ray diffractometer (XRD, Rigaku, D/ Max 2500PC). Specific test parameters: Cu target Ka radiation, characteristic wavelength λ=0.154056 nm, diffraction Angle (2θ) scanning speed of 0.02 °/s, scanning range of 20 ° -80 °, current of 100 mA, voltage of 40 KV.