采用0.8μm的钨粉压制出试棒,分别在2000℃和2300℃进行氢气烧结,对烧结出的钨棒进行金相组织观察。金相组织采集方案:试样经过机械磨削和抛光成平整、光亮、无磨痕或抛光划痕的镜面,采用10-20%的氢氧化钠+铁氰化钾混合液(氢氧化钠与铁氰化钾质量比为1:1)对样品进行腐蚀,腐蚀后的样品在金相显微镜下放大100×或200×进行金相组织观察。
Test rods were pressed by 0.8μm tungsten powder, and hydrogen sintering was performed at 2000°C and 2300°C respectively, and the metallographic structure of the sintered tungsten rods was observed. Metallographic structure collection scheme: The sample is mechanically ground and polished into a smooth, bright, and non-abrasive or polished mirror surface, using a 10-20% sodium hydroxide + potassium ferricyanide mixture (sodium hydroxide and potassium ferricyanide) The mass ratio of potassium ferricyanide is 1:1) The sample is corroded, and the corroded sample is magnified 100× or 200× under a metallurgical microscope to observe the metallographic structure.