一种制备纯铼金属零部件的方法,属于粉末冶金技术领域。首先采用对喷式气流磨装置将原料铼粉进行二次气流磨技术处理,得到流动性良好、分散均匀、窄粒径分布的近球形铼粉,以使其可直接供选区激光熔化(SLM)成形使用。然后将铼粉在氢气气氛下还原处理以降低其氧含量,提升其烧结活性。同时,通过计算机建模软件设计出复杂形状的铼金属零部件的三维示意图并设置最优的加工参数(如扫描速度、扫描间距、扫描层厚和扫描方向等),导出参数文件实现建模。最后将粉末进行选区激光熔化成形,制备出复杂形状的铼金属零部件。该发明显著提高了原料粉末的球形度、流动性和烧结活性,并优化了选区激光熔化(SLM)加工参数,制备出的铼金属零部件件氧含量低且接近完全致密。
A method for preparing pure rhenium metal parts belongs to the technical field of powder metallurgy. First, a jet mill device is used to process the raw rhenium powder with secondary jet milling technology to obtain a nearly spherical rhenium powder with good fluidity, uniform dispersion and narrow particle size distribution, so that it can be directly used for selective laser melting (SLM) Forming use. Then the rhenium powder is reduced in a hydrogen atmosphere to reduce its oxygen content and improve its sintering activity. At the same time, the three-dimensional schematic diagram of the complex-shaped rhenium metal parts is designed through computer modeling software and the optimal processing parameters (such as scanning speed, scanning distance, scanning layer thickness and scanning direction, etc.) are set, and parameter files are exported to realize modeling. Finally, the powder is laser-melted and formed into a selected area to prepare rhenium metal parts with complex shapes. The invention significantly improves the sphericity, fluidity and sintering activity of the raw material powder, and optimizes the selective laser melting (SLM) processing parameters, and the prepared rhenium metal parts have low oxygen content and are nearly completely dense.