本课题围绕“研究低温、高压服役条件下高强度管线钢的断裂力学行为和韧化机理,阐明低温条件下控制韧性断裂和止裂的物理冶金学原理”和“建立低温超大输量管道用钢的理论体系”等相关内容开展研究。经过4年的研发,解决了“低温X80管线钢、焊缝和热区断裂机制及韧性止裂的冶金学原理”这一主要科学问题。突破了“低温厚规格X80钢板/带成分设计及相变控制技术”、“低温用厚壁X80钢管焊接接头韧化控制技术”两项共性关键技术。开展了“X80管线钢低温断裂韧性控制的金属学原理研究”、“超宽厚钢板/带成分设计、相变动力学及组织精细化控制技术”、“钢管埋弧焊缝和热区精细组织特征与低温韧性关系”“X80钢管环焊缝韧化控制技术”四项主要内容的研究。取得主要结论如下:国际上率先提出了管线钢中变形奥氏体的尺寸控制与DWTT性能的相关性,奠定了解决厚规格DWTT性能控制难题的理论基础;开发了“粗轧低温快轧”创新技术,实现了我国厚规格管线钢生产的重大技术突破;开发了“超细晶铁素体+针状铁素体”新一代高钢级管线钢制造技术,为我国特厚规格管线钢发展奠定基础;揭示了自保护焊缝韧性波动的致因,阐明了多层多道焊缝各区域的强韧化特征,研发了高Ni系列的高强韧X80自保护焊丝,相比于原成分体系焊丝对母材化学成分具有更高的适应性;在国内首次提出了基于良好焊接性的低温X80管线钢成分设计,该成分设计有效指导了中俄东线管道工程技术条件的制定。
This subject was focused on: study of the fracture mechanics and toughening mechanism of high-strength pipeline steel under the low temperature and high pressure service conditions; clarify the principles of the physical metallurgy to control ductile fracture and arrest under the low temperature conditions; establish a theoretical system for steel used in the low-temperature and super-large-volume pipelines. After 4 years of research and development, the main scientific problem of "the weld and hot zone fracture mechanism and toughness crack arrest metallurgy principle of the low temperature X80 pipeline steel" had been solved. The two common key technologies of "composition design and phase transformation control technology of the low temperature thick X80 steel plate/strip" and " toughening control technology of the welded joint of the low temperature thick wall X80 steel pipe" were broken through. Four main contents of research “metallurgical principles of low temperature fracture toughness control of X80 pipeline steel”, “fine control technology of ultra-wide thick steel plate/belt composition design, phase change dynamics and microstructure”, “the relationship among fine structure characteristics of steel pipe submerged arc weld, hot zone and low temperature toughness”, “toughening control technology of X80 steel pipe girth weld” were carried out. The main conclusions are as follows: The correlation between the grain size control of the deformed austenite in pipeline steel and the performance of DWTT was first proposed in the world, which provided a theoretical foundation to solve the problem of the DWTT performance control with thick specifications. The innovative technology of "low temperature and fast rough rolling" was developed, which realized a major technological breakthrough in the production of thick-size pipeline steel in our country. A new generation of manufacturing technology of high-grade pipeline steel with "ultra-fine ferrite + acicular ferrite" was developed. The cause of the self-shielded welds was discovered. The characteristics of the strengthening and toughening in each zone of the multi-layer and multi-pass welds were clarified. The high-strength X80 self-shielded welding wire of high Ni series was developed. The welding wire had higher adaptability to the chemical composition of the base metal compared with the original composition system. The composition design of the low temperature X80 pipeline steel based on good weldability was proposed for the first time in China. This component design effectively guided the formulation of technical conditions for the China-Russia eastern natural gas pipeline engineering.