该数据为放大反应底物原料的加量,以80mmol的氯化苄基喹啉季铵盐为原料,反应物3eq.的NaNO2作为氧化剂,异丙醇作为溶剂,在140℃下反应4h,考察反应底物浓度对合成产物的影响,同时检测粗产品中衍生物的含量。
The data were used to amplify the addition of the reaction substrate feedstock, 80 mmol of benzyl quinoline quaternary ammonium chloride as feedstock, 3eq. of NaNO2 as oxidizer and isopropanol as solvent, and the reaction was carried out at 140 °C for 4 h. The effect of the reaction substrate concentration on the synthesized products was investigated, and the amount of derivatives in the crude product was also assayed.