以0.2mmol的氯化苄基喹啉季铵盐为原料,反应物3eq.的NaNO2作为氧化剂,在140℃下反应4h,考察不同溶剂对合成产物的影响,同时检测粗产品中衍生物的含量。
The reaction was carried out with 0.2 mmol of benzyl quinolinium chloride quaternary ammonium salt as raw material and 3 eq. of NaNO2 as oxidizing agent at 140 °C for 4 h. The effect of different solvents on the synthesized products was investigated, and the amount of derivatives in the crude product was also detected.