通过对BQD进行复配性能及机理研究,进一步提高了BQD的缓蚀性能,优选出合适的复配剂。通过对增效剂进行筛选,溶剂筛查,改变复配配方比例确定最优的复配配方,其中通过静态失重法进行评价,最终得到DS-1缓蚀剂体系。主要采用磁上海市卓精电子科技有限公司电子天平,海泰科技磁力加热搅拌器,上海高鸽工贸有限公司10μL微量移液器,予华仪器有限责任公司循环水式真空泵SHZ(Ⅲ),上海亚荣生化仪器厂旋转蒸发器RE52CS-2等设备。该数据为在90℃、20 wt.%盐酸溶液中,以BQD纯品为主剂,在复配剂浓度不变时,选择不同添加剂(CTAB、SDS、乌洛托品、KI、SbCl3)进行复配增效研究,优选合适的复配剂后续的缓蚀剂配方提供借鉴。
The corrosion inhibition performance of BQD was further improved by compounding performance and mechanism study, and suitable compounding agent was preferred. The optimal compounding formula was determined by screening the synergist, solvent screening, and changing the ratio of the compounding formula, which was evaluated by the static weight loss method, and finally the DS-1 corrosion inhibitor system was obtained. mainly uses magnetic Shanghai Zhuojing Electronic Technology Co., Ltd. electronic balance, Haitai Technology magnetic heating stirrer, Shanghai Gaoge Industry and Trade Co., Ltd. 10μL micro pipette, Yuhua Instrument Co., Ltd. circulating water vacuum pump SHZ (III.), Shanghai Yarong Biochemical Instrument Factory rotary evaporator RE52CS-2 and other equipment.The data provide a reference for the study of compounding potentiation by selecting different additives (CTAB, SDS, urotropin, KI, SbCl3) in 90°C, 20 wt.% hydrochloric acid solution with BQD pure product as the main agent, and the selection of a suitable compound for subsequent corrosion inhibitor formulation when the concentration of the compounding agent is unchanged.