合成路径优化主要采用磁上海市卓精电子科技有限公司电子天平,海泰坦科技磁力加热搅拌器,上海高鸽工贸有限公司10 μL微量移液器,予华仪器有限责任公司循环水式真空泵SHZ-D(III),上海亚荣生化仪器厂旋转蒸发器RE52CS-2等设备。该数据为考察不同氧化剂及加量对合成反应的影响,使用核磁共振氢谱方法检测粗产品中氯化苄基喹啉季铵盐衍生物的含量。
The synthetic pathway optimization mainly used magnetic Shanghai Zhuojing Electronic Technology Co., Ltd. electronic balance, Haitaitan Technology magnetic heating stirrer, Shanghai Gaofei Industry and Trade Co., Ltd. 10 μL micropipette, Yuhua Instrument Co., Ltd. recirculating water vacuum pump SHZ-D (III), Shanghai Yarong Biochemical Instrument Factory rotary evaporator RE52CS-2 and other equipment.Examination of the effects of different oxidizing agents and addition amounts on the synthesis reaction, and simultaneous determination of benzylquinoline quaternary ammonium chloride derivatives in the crude product by nuclear magnetic resonance hydrogen spectrometry