本发明属于气体传感器与环境检测技术领 域,具体涉及一种基于Fe‑MOF材料衍生的α‑Fe2O3丙酮气体传感材料的制备方法。一种Fe-MOF衍生的α‑Fe2O3丙酮气体传感材料的制备方法,室温下,将NH3·H2O与H3BTC于去离子水中混合均匀,记为溶液A;将FeCl2溶液在室温条件下缓慢滴加入A溶液中,得到橙红色的悬浊液,离心,烘干,清洗,最后用NH4F溶液进行化学处理,干燥,焙烧。本发明制备的α‑Fe2O3传感材料具有良好的气敏性能,选择性能优秀,能明显筛分 出丙酮与其它气体。本发明制备的α‑Fe2O3传感器的检出限低,能达到ppm级别,稳定性高,可满足早期糖尿病预防的长期检测需求。
The present invention belongs to the field of gas sensors and environmental detection technology, and specifically relates to a derivative based on Fe-MOF materials α‑Fe2O3 acetone gas sensing material. A Fe-MOF derivative α‑Fe2O3 acetone gas sensing material, at room temperature, NH3·H2O and H3BTC are uniformly mixed in deionized water, denoted as solution A; Slowly add FeCl2 solution to solution A at room temperature to obtain an orange red suspension. Centrifuge, dry, clean, and finally chemically treat with NH4F solution, dry, and calcine. The present invention is prepared α‑Fe2O3 sensing material has good gas sensing performance, excellent selectivity, and can clearly screen out acetone and other gases. The present invention is prepared α‑Fe2O3 sensor has a low detection limit, can reach the ppm level, and has high stability, which can meet the long-term detection needs of early diabetes prevention.